endobj Accelerated Solvent Extraction (ASE) and High-Temperature Water Extraction. 118 0 obj <>stream X>. Valeria Nardelli, Valeria D’Amico, Francesco Casamassima, Giuseppe Gesualdo, Donghao Li, Wadir M.V. Your Mendeley pairing has expired. Critical overview of selected contemporary sample preparation techniques. %PDF-1.5 Analysis of omega-3 fatty acids in foods and supplements. %PDF-1.6 %���� Li-Chun Zhao, Ying He, Xin Deng, Geng-Liang Yang, Wei Li, Jian Liang, Qian-Li Tang. Chemical Composition of Date Pits: Potential to Extract and Characterize the Lipid Fraction. It is difficult to pursue direct ASE with acid- or base-hydrolyzed samples due to the corrosive nature of the reagents and material limitations. x��X_o�8���Giq�E���C! Rapid Determination of Fat, Protein and Amino Acid Content in Coix Seed Using Near-Infrared Spectroscopy Technique. Get article recommendations from ACS based on references in your Mendeley library. Victor H. M. da Cruz, Rafael L. G. Priori, Patrícia D. S. Santos, Cintia S. F. Ferreira, Angélica de F. B. Piccioli, Roberta da Silveira, Jesuí V. Visentainer, Oscar O. Santos. You have to login with your ACS ID befor you can login with your Mendeley account. 13 publications. stream endstream endobj startxref Chang. baked and extruded products and pet foods) require acid to breakdown the fats (e.g. '���ɼ,�&۾]^�L2��T*�X�D2�d"$[��/��MS��{���� s��jy��T�"-����-�����J&�,�+LJ��g1��e9��)˔ʒ4;��zE)�]^�ä8��Ce@�,��!&7����a�e?�sY�Q�[��3+ A��k�x]�Y�K�5^�~�U���[x�F�phq}���Y�SF@QJ>�ӑO�>)0*��TB6�����!+����x�^���`��l����>V��z �Q����l�)��ϸ���>�������l��?��y��?r����ۓ��Q�l@�D?��v�� ��y���'r�g�L�TbOhH��X�Rhg��SIb}VIe|��?99��UF��(. Extraction and Liquid Chromatography–Tandem Mass Spectrometry Detection of 3-Monochloropropanediol Esters and Glycidyl Esters in Infant Formula. ]ͨ#�VIr��m�2��QU��Z` the Altmetric Attention Score and how the score is calculated. Experimental investigation on cleaner process of enhanced fat-oil extraction from alkaline leather fleshing waste. 3 0 obj The acid hydrolysis method is applicable to baked products and pet foods, and facilitates the extraction of fatty acids from glycerides, glycolipids and phospholipids and sterol esters that might otherwise be left un-extracted due to covalent and ionic bonding. Page 1 of 1 F419 Crude Fat (Acid Hydrolysis) Samples containing complexed/bound lipids or fats (e.g. h�bbd```b``���@$�0[D2��H�G`�i �UL��e���4��u�E l&X�,����sg�mi��kA$X�l�$�%� ���l/��} ��f4��l�6 ���g&����a`��&�� ;F� 1 0 obj Development of a screening analytical method for the determination of non-dioxin-like polychlorinated biphenyls in chicken eggs by gas chromatography and electron capture detection. Transgenic soya bean seeds accumulating β-carotene exhibit the collateral enhancements of oleate and protein content traits. Kubendran Devaraj, Salma Aathika, Yuvarai Mani, Amudha Thanarasu, Karthik Periyasamy, Premkumar Periyaraman, Karthikeyan Velayutham, Sivanesan Subramanian. endobj <> Chemical Printing of Biological Tissue by Gold Nanoparticle-Assisted Laser Ablation. endstream endobj 51 0 obj <>>>/Filter/Standard/Length 128/O(�ռJ����6l\(lb�� �iel�Bou����)/P -1036/R 4/StmF/StdCF/StrF/StdCF/U(��S� )/V 4>> endobj 52 0 obj <>>> endobj 53 0 obj <> endobj 54 0 obj <>/ExtGState<>/Font<>/Pattern<>/ProcSet[/PDF/Text]/Properties<>>>/Rotate 0/TrimBox[0.0 0.0 594.0 792.0]/Type/Page>> endobj 55 0 obj <>stream fat extraction acid hydrolysis base hydrolysis gravimetry fat analysis sample preparation Cited By This article is cited by 12 publications. Excellent fat recoveries were obtained for the ASE methods. Extraction of Total Fat from Food Samples After Acid Hydrolysis Using Accelerated Solvent Extraction with GC-MS Analysis Brett Murphy, Brian Dorich, and Bruce Richter Thermo Fisher Scientific, Salt Lake City, UT, USA Application Note 361 Introduction Sample z@#�=O}�6O� ���*���;�OK$�١ q���oC#�br&��Td�lHD�#B ��X)X(�i������pʕhӦf��Jp&. � VR�O����Ҫ�|y�%b,����zy�X&8�E���/ѧx�G�XD�.c&v'�9� w�I��v�o����'�s���L-�*{]��~�B���LD�:��{�&tey$y!x�vd�H! Application Note 361 Extraction of Total Fat from Food Samples After Acid Hydrolysis Using Accelerated Solvent Extraction (ASE) with GC-MS Analysis IntroductIon Sample preparation—specifically, solvent extraction—is an important step in the analytical process. Find more information about Crossref citation counts. endobj I�]���5o�>8���ة���o�3�"e+�6d����͈l���{7�x��{��5�~��?�ls���lsy��Y��UU�)�%�^���������#l����~���U�/W͚}�_��~������S3��ܴ�e��w���w=.-�������ˋ���L$�b���@ 4 0 obj 85 0 obj <>/Encrypt 51 0 R/Filter/FlateDecode/ID[<4A7E2C81B93F6447AAD8A4D4D88F0621>]/Index[50 69]/Info 49 0 R/Length 142/Prev 186785/Root 52 0 R/Size 119/Type/XRef/W[1 3 1]>>stream Marchesiello, Donatella Nardiello, Maurizio Quinto. Clicking on the donut icon will load a page at altmetric.com with additional details about the score and the social media presence for the given article. Please note: If you switch to a different device, you may be asked to login again with only your ACS ID. According to Joslyn (1970) , the extracted fat percentage of dried egg, flour, noodles, and semolina was increased by 1–6% due to pre acid digestion. Monica A. Schmidt, Wayne A. Parrott, David F. Hildebrand, R. Howard Berg, Amanda Cooksey, Ken Pendarvis, Yonghua He, Fiona McCarthy, Eliot M. Herman. Abstract The extraction efficiency of Soxhlet, acid hydrolysis and Bligh and Dyer were evaluated by using direct methylation on extracts and residues for calculating the mass balance of fatty acids for eight marine powders (fishmeals, krillmeals, cod filet, salmon filet Please reconnect. In this study ion exchange based materials were used to remove acid or base reagents in-cell without compromising the recovery of lipids. Physicochemical properties and storage stability of soybean protein nanoemulsions prepared by ultra-high pressure homogenization. 2 0 obj You’ve supercharged your research process with ACS and Mendeley! Response Surface Modeling and Optimization of Accelerated Solvent Extraction of Four Lignans from Fructus Schisandrae. Find more information about Crossref citation counts. Fat Extraction from Acid- and Base-Hydrolyzed Food Samples Using Accelerated Solvent Extraction, Dionex Corporation, 445 Lakeside Drive, Sunnyvale, California 94085, United States, SLC Technical Center, Dionex Corporation, Suite A, 1182 West 2400 South, Salt Lake City, Utah 84119, United States. 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acid hydrolysis fat extraction

Xing Liu, Xin Zhang, Yu-Zhi Rong, Jin-Hong Wu, Yong-Jian Yang, Zheng-Wu Wang. <> %%EOF endobj +%v����QN��S�#���f?3;�۳�I_S�cS��ώ�������Z�]W�MC?�c!��>/8^��h���֗�����ʗ�+�"2�A��&�2���&Y�P#�R������E��%���#��Rg- �d�����N�q��\M�$�H����n7��'R����B���L�m[]����c8k S-��}�ݾA�W 50 0 obj <> endobj Accelerated Solvent Extraction (ASE) and High-Temperature Water Extraction. 118 0 obj <>stream X>. Valeria Nardelli, Valeria D’Amico, Francesco Casamassima, Giuseppe Gesualdo, Donghao Li, Wadir M.V. Your Mendeley pairing has expired. Critical overview of selected contemporary sample preparation techniques. %PDF-1.5 Analysis of omega-3 fatty acids in foods and supplements. %PDF-1.6 %���� Li-Chun Zhao, Ying He, Xin Deng, Geng-Liang Yang, Wei Li, Jian Liang, Qian-Li Tang. Chemical Composition of Date Pits: Potential to Extract and Characterize the Lipid Fraction. It is difficult to pursue direct ASE with acid- or base-hydrolyzed samples due to the corrosive nature of the reagents and material limitations. x��X_o�8���Giq�E���C! Rapid Determination of Fat, Protein and Amino Acid Content in Coix Seed Using Near-Infrared Spectroscopy Technique. Get article recommendations from ACS based on references in your Mendeley library. Victor H. M. da Cruz, Rafael L. G. Priori, Patrícia D. S. Santos, Cintia S. F. Ferreira, Angélica de F. B. Piccioli, Roberta da Silveira, Jesuí V. Visentainer, Oscar O. Santos. You have to login with your ACS ID befor you can login with your Mendeley account. 13 publications. stream endstream endobj startxref Chang. baked and extruded products and pet foods) require acid to breakdown the fats (e.g. '���ɼ,�&۾]^�L2��T*�X�D2�d"$[��/��MS��{���� s��jy��T�"-����-�����J&�,�+LJ��g1��e9��)˔ʒ4;��zE)�]^�ä8��Ce@�,��!&7����a�e?�sY�Q�[��3+ A��k�x]�Y�K�5^�~�U���[x�F�phq}���Y�SF@QJ>�ӑO�>)0*��TB6�����!+����x�^���`��l����>V��z �Q����l�)��ϸ���>�������l��?��y��?r����ۓ��Q�l@�D?��v�� ��y���'r�g�L�TbOhH��X�Rhg��SIb}VIe|��?99��UF��(. Extraction and Liquid Chromatography–Tandem Mass Spectrometry Detection of 3-Monochloropropanediol Esters and Glycidyl Esters in Infant Formula. ]ͨ#�VIr��m�2��QU��Z` the Altmetric Attention Score and how the score is calculated. Experimental investigation on cleaner process of enhanced fat-oil extraction from alkaline leather fleshing waste. 3 0 obj The acid hydrolysis method is applicable to baked products and pet foods, and facilitates the extraction of fatty acids from glycerides, glycolipids and phospholipids and sterol esters that might otherwise be left un-extracted due to covalent and ionic bonding. Page 1 of 1 F419 Crude Fat (Acid Hydrolysis) Samples containing complexed/bound lipids or fats (e.g. h�bbd```b``���@$�0[D2��H�G`�i �UL��e���4��u�E l&X�,����sg�mi��kA$X�l�$�%� ���l/��} ��f4��l�6 ���g&����a`��&�� ;F� 1 0 obj Development of a screening analytical method for the determination of non-dioxin-like polychlorinated biphenyls in chicken eggs by gas chromatography and electron capture detection. Transgenic soya bean seeds accumulating β-carotene exhibit the collateral enhancements of oleate and protein content traits. Kubendran Devaraj, Salma Aathika, Yuvarai Mani, Amudha Thanarasu, Karthik Periyasamy, Premkumar Periyaraman, Karthikeyan Velayutham, Sivanesan Subramanian. endobj <> Chemical Printing of Biological Tissue by Gold Nanoparticle-Assisted Laser Ablation. endstream endobj 51 0 obj <>>>/Filter/Standard/Length 128/O(�ռJ����6l\(lb�� �iel�Bou����)/P -1036/R 4/StmF/StdCF/StrF/StdCF/U(��S� )/V 4>> endobj 52 0 obj <>>> endobj 53 0 obj <> endobj 54 0 obj <>/ExtGState<>/Font<>/Pattern<>/ProcSet[/PDF/Text]/Properties<>>>/Rotate 0/TrimBox[0.0 0.0 594.0 792.0]/Type/Page>> endobj 55 0 obj <>stream fat extraction acid hydrolysis base hydrolysis gravimetry fat analysis sample preparation Cited By This article is cited by 12 publications. Excellent fat recoveries were obtained for the ASE methods. Extraction of Total Fat from Food Samples After Acid Hydrolysis Using Accelerated Solvent Extraction with GC-MS Analysis Brett Murphy, Brian Dorich, and Bruce Richter Thermo Fisher Scientific, Salt Lake City, UT, USA Application Note 361 Introduction Sample z@#�=O}�6O� ���*���;�OK$�١ q���oC#�br&��Td�lHD�#B ��X)X(�i������pʕhӦf��Jp&. � VR�O����Ҫ�|y�%b,����zy�X&8�E���/ѧx�G�XD�.c&v'�9� w�I��v�o����'�s���L-�*{]��~�B���LD�:��{�&tey$y!x�vd�H! Application Note 361 Extraction of Total Fat from Food Samples After Acid Hydrolysis Using Accelerated Solvent Extraction (ASE) with GC-MS Analysis IntroductIon Sample preparation—specifically, solvent extraction—is an important step in the analytical process. Find more information about Crossref citation counts. endobj I�]���5o�>8���ة���o�3�"e+�6d����͈l���{7�x��{��5�~��?�ls���lsy��Y��UU�)�%�^���������#l����~���U�/W͚}�_��~������S3��ܴ�e��w���w=.-�������ˋ���L$�b���@ 4 0 obj 85 0 obj <>/Encrypt 51 0 R/Filter/FlateDecode/ID[<4A7E2C81B93F6447AAD8A4D4D88F0621>]/Index[50 69]/Info 49 0 R/Length 142/Prev 186785/Root 52 0 R/Size 119/Type/XRef/W[1 3 1]>>stream Marchesiello, Donatella Nardiello, Maurizio Quinto. Clicking on the donut icon will load a page at altmetric.com with additional details about the score and the social media presence for the given article. Please note: If you switch to a different device, you may be asked to login again with only your ACS ID. According to Joslyn (1970) , the extracted fat percentage of dried egg, flour, noodles, and semolina was increased by 1–6% due to pre acid digestion. Monica A. Schmidt, Wayne A. Parrott, David F. Hildebrand, R. Howard Berg, Amanda Cooksey, Ken Pendarvis, Yonghua He, Fiona McCarthy, Eliot M. Herman. Abstract The extraction efficiency of Soxhlet, acid hydrolysis and Bligh and Dyer were evaluated by using direct methylation on extracts and residues for calculating the mass balance of fatty acids for eight marine powders (fishmeals, krillmeals, cod filet, salmon filet Please reconnect. In this study ion exchange based materials were used to remove acid or base reagents in-cell without compromising the recovery of lipids. Physicochemical properties and storage stability of soybean protein nanoemulsions prepared by ultra-high pressure homogenization. 2 0 obj You’ve supercharged your research process with ACS and Mendeley! Response Surface Modeling and Optimization of Accelerated Solvent Extraction of Four Lignans from Fructus Schisandrae. Find more information about Crossref citation counts. Fat Extraction from Acid- and Base-Hydrolyzed Food Samples Using Accelerated Solvent Extraction, Dionex Corporation, 445 Lakeside Drive, Sunnyvale, California 94085, United States, SLC Technical Center, Dionex Corporation, Suite A, 1182 West 2400 South, Salt Lake City, Utah 84119, United States.

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